4J77
Crystal structure of beta'-COP/hWbp1 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Detector technology | CCD |
Detector | ADSC QUANTUM 315 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 75.681, 50.935, 82.421 |
Unit cell angles | 90.00, 90.24, 90.00 |
Refinement procedure
Resolution | 36.129 - 1.756 |
R-factor | 0.2032 |
Rwork | 0.202 |
R-free | 0.24510 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.013 |
RMSD bond angle | 1.557 |
Refinement software | PHENIX ((phenix.refine: 1.8_1069)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 75.680 |
High resolution limit [Å] | 1.756 |
Number of reflections | 60204 |
Completeness [%] | 97.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |