4J73
Crystal structure of beta'-COP/p25 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Detector technology | CCD |
Detector | ADSC QUANTUM 315 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 36.295, 56.696, 132.352 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 31.823 - 1.439 |
R-factor | 0.1783 |
Rwork | 0.177 |
R-free | 0.20070 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.011 |
RMSD bond angle | 1.471 |
Refinement software | PHENIX ((phenix.refine: 1.8_1069)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 66.176 |
High resolution limit [Å] | 1.439 |
Number of reflections | 48785 |
Completeness [%] | 96.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |