4J4U

Pentamer SFTSVN

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL17U
Synchrotron site	SSRF
Beamline	BL17U
Temperature [K]	100
Detector technology	CCD
Collection date	2011-11-26
Detector	ADSC QUANTUM 315
Wavelength(s)	0.98
Spacegroup name	C 1 2 1
Unit cell lengths	111.188, 155.573, 97.656
Unit cell angles	90.00, 107.52, 90.00

Refinement procedure

Resolution	43.808 - 2.803
R-factor	0.1998
Rwork	0.195
R-free	0.27900
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	4j4r
RMSD bond length	0.010
RMSD bond angle	1.236
Refinement software	PHENIX ((phenix.refine: 1.8.1_1168))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	43.810	2.900
High resolution limit [Å]	2.800	2.800
Number of reflections	38804
Completeness [%]	92.5	92.4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1