4J2N
Crystal Structure of mycobacteriophage Pukovnik Xis
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E DW |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-07-15 |
Detector | RIGAKU SATURN 944 |
Wavelength(s) | 1.5418 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 89.423, 129.985, 92.346 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 35.921 - 2.348 |
R-factor | 0.2294 |
Rwork | 0.226 |
R-free | 0.26700 |
Structure solution method | SAD |
RMSD bond length | 0.007 |
RMSD bond angle | 0.984 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHENIX (1.6.1_357) |
Refinement software | PHENIX (1.6.1_357) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 90.000 | 2.390 |
High resolution limit [Å] | 2.350 | 2.350 |
Number of reflections | 22815 | |
<I/σ(I)> | 2.2 | |
Completeness [%] | 99.8 | 100 |
Redundancy | 4.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 300 | ammonium sulfate, PEG 3350, pH 8.0, VAPOR DIFFUSION, SITTING DROP, temperature 300K |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 300 | ammonium sulfate, PEG 3350, pH 8.0, VAPOR DIFFUSION, SITTING DROP, temperature 300K |