4J2G
Atg13 HORMA domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I02 |
Synchrotron site | Diamond |
Beamline | I02 |
Temperature [K] | 200 |
Detector technology | PIXEL |
Collection date | 2012-05-28 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 1.0 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 118.650, 65.670, 85.760 |
Unit cell angles | 90.00, 101.46, 90.00 |
Refinement procedure
Resolution | 57.250 - 2.290 |
R-factor | 0.21689 |
Rwork | 0.214 |
R-free | 0.26279 |
Structure solution method | SAD |
RMSD bond length | 0.017 |
RMSD bond angle | 2.052 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | SHELXS |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 84.050 |
High resolution limit [Å] | 2.290 |
Completeness [%] | 99.0 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 294 | 0.2mM ammonium sulfate, 0.1M MES pH6.5, 20% w/v PEG 8000, VAPOR DIFFUSION, HANGING DROP, temperature 294K |