4IWJ
Crystal structure of iron soaked (45 min) ferritin from Pseudo-nitzschia multiseries
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL7-1 |
Synchrotron site | SSRL |
Beamline | BL7-1 |
Detector technology | CCD |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1 |
Spacegroup name | P 2 3 |
Unit cell lengths | 175.319, 175.319, 175.319 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 41.360 - 1.950 |
R-factor | 0.1749 |
Rwork | 0.173 |
R-free | 0.21330 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.024 |
RMSD bond angle | 2.060 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | REFMAC |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.020 |
High resolution limit [Å] | 1.950 | 4.200 | 1.950 |
Rmerge | 0.064 | 0.027 | 0.528 |
Number of reflections | 129748 | ||
<I/σ(I)> | 16.1 | ||
Completeness [%] | 100.0 | 99.6 | 100 |
Redundancy | 11.6 | 14.3 | 7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | pH 5.5, VAPOR DIFFUSION, HANGING DROP |