4IT3
Crystal Structure of Iml3 from S. cerevisiae
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Temperature [K] | 77 |
Detector technology | CCD |
Collection date | 2012-02-19 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.97919 |
Spacegroup name | P 63 2 2 |
Unit cell lengths | 73.135, 73.135, 189.133 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 37.889 - 2.495 |
R-factor | 0.2269 |
Rwork | 0.224 |
R-free | 0.25560 |
Structure solution method | SAD |
RMSD bond length | 0.004 |
RMSD bond angle | 0.808 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHENIX |
Refinement software | PHENIX (1.8.1_1168) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 37.889 | 37.889 | 2.540 |
High resolution limit [Å] | 2.494 | 6.780 | 2.494 |
Rmerge | 0.103 | 0.061 | 0.876 |
Number of reflections | 11048 | ||
<I/σ(I)> | 10.2 | ||
Completeness [%] | 99.5 | 96.6 | 99.4 |
Redundancy | 12.7 | 9.2 | 13.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 291 | 3.75 M sodium formate, 4% 2,5-diaminopentane, pH 8.5, VAPOR DIFFUSION, HANGING DROP, temperature 291K |