4ISP
Crystal structure of iron soaked (4h) ferritin from Pseudo-nitzschia multiseries
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL7-1 |
Synchrotron site | SSRL |
Beamline | BL7-1 |
Detector technology | CCD |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1 |
Spacegroup name | P 2 3 |
Unit cell lengths | 175.446, 175.446, 175.446 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 42.590 - 2.200 |
R-factor | 0.19 |
Rwork | 0.187 |
R-free | 0.24220 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.019 |
RMSD bond angle | 1.911 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | REFMAC |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.280 |
High resolution limit [Å] | 2.200 | 4.740 | 2.200 |
Rmerge | 0.122 | 0.048 | 0.553 |
Number of reflections | 90690 | ||
<I/σ(I)> | 8.4 | ||
Completeness [%] | 100.0 | 99.9 | 100 |
Redundancy | 14 | 14.4 | 12 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |