4IPE
Crystal structure of mitochondrial Hsp90 (TRAP1) with AMPPNP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.3.1 |
Synchrotron site | ALS |
Beamline | 8.3.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-04-12 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.115869 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 177.977, 96.362, 125.153 |
Unit cell angles | 90.00, 134.34, 90.00 |
Refinement procedure
Resolution | 26.240 - 2.289 |
R-factor | 0.1811 |
Rwork | 0.180 |
R-free | 0.22460 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.161 |
Data reduction software | HKL-2000 |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: dev_1214)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 35.000 | 2.380 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.068 | 0.060 |
Number of reflections | 67287 | |
<I/σ(I)> | 1.7 | |
Completeness [%] | 99.5 | 98.2 |
Redundancy | 3.1 | 3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.6 | 296 | 0.2M Sodium Malonate pH 6.6, 18% (v/v) PEG 3350, 20uM hexamine cobalt, VAPOR DIFFUSION, HANGING DROP, temperature 296K |