4IOL
N10-formyltetrahydrofolate synthetase from Moorella thermoacetica with ADP/ZD9 and XPO
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Temperature [K] | 100 |
Spacegroup name | H 3 2 |
Unit cell lengths | 160.370, 160.370, 258.074 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 122.300 - 2.563 |
R-factor | 0.19442 |
Rwork | 0.190 |
R-free | 0.27916 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3SIN |
RMSD bond length | 0.010 |
RMSD bond angle | 1.560 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 122.300 |
High resolution limit [Å] | 2.560 |
Rmerge | 0.049 |
Number of reflections | 79627 |
<I/σ(I)> | 9.4 |
Completeness [%] | 91.1 |
Redundancy | 4.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 298 | 18 to 22% (w/v) PEG 6-8K, 0.2M AS, 1 mM DTT, 75 mM KMB pH 7.0-8.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |