4IKE
Crystal Structure of a partly open ATP-lid of liganded Adenylate kinase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.2.1 |
Synchrotron site | ALS |
Beamline | 8.2.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-05-20 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.999800 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 56.370, 61.570, 58.890 |
Unit cell angles | 90.00, 94.33, 90.00 |
Refinement procedure
Resolution | 33.040 - 1.480 |
R-factor | 0.1629 |
Rwork | 0.161 |
R-free | 0.19800 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 1.141 |
Data reduction software | iMOSFLM |
Data scaling software | SCALA |
Phasing software | AutoBuild |
Refinement software | PHENIX ((phenix.refine: dev_1039)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 34.820 |
High resolution limit [Å] | 1.480 |
Rmerge | 0.076 |
Number of reflections | 66831 |
Completeness [%] | 99.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.2 | 295 | pH 5.2, VAPOR DIFFUSION, SITTING DROP, temperature 295K |