4IKA
Crystal structure of EV71 3Dpol-VPg
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BSRF BEAMLINE 3W1A |
Synchrotron site | BSRF |
Beamline | 3W1A |
Detector technology | CCD |
Collection date | 2010-01-15 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 1.0000 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 103.596, 103.596, 132.170 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 48.227 - 2.700 |
R-factor | 0.2213 |
Rwork | 0.218 |
R-free | 0.27750 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3n6l |
RMSD bond length | 0.008 |
RMSD bond angle | 1.217 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX ((phenix.refine: 1.7.1_743)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 2.700 |
Number of reflections | 22929 |
Completeness [%] | 96.0 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.1 | 291 | 1.3M ammonium sulfate, 0.1M Bis-Tris (pH 6.1), 1mM DTT, 10mM NiCl2 , VAPOR DIFFUSION, HANGING DROP, temperature 291K |