4IIP
Legionella pneumophila effector
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I24 |
Synchrotron site | Diamond |
Beamline | I24 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2011-02-28 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 60.532, 71.422, 88.185 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 28.630 - 1.900 |
R-factor | 0.1515 |
Rwork | 0.149 |
R-free | 0.19340 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.019 |
RMSD bond angle | 1.884 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP |
Refinement software | REFMAC |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 28.630 | 2.010 | |
High resolution limit [Å] | 1.900 | 5.600 | 1.900 |
Rmerge | 0.090 | 0.035 | 0.524 |
Rmeas | 0.097 | 0.038 | 0.566 |
Number of reflections | 30812 | 1310 | 4815 |
<I/σ(I)> | 18.18 | 46.32 | 4.53 |
Completeness [%] | 99.6 | 99.1 | 98.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4.8 | 291 | 1.6M NaCl, 0.1M Na acetate, pH 4.8, VAPOR DIFFUSION, SITTING DROP, temperature 291K |