4IHN
High Resolution Insulin by Langmuir-Blodgett Modified Hanging Drop Vapour Diffusion
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-4 |
Synchrotron site | ESRF |
Beamline | ID14-4 |
Detector technology | CCD |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9395 |
Spacegroup name | I 21 3 |
Unit cell lengths | 78.340, 78.340, 78.340 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 55.390 - 1.160 |
R-factor | 0.2343 |
Rwork | 0.233 |
R-free | 0.26000 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.035 |
RMSD bond angle | 2.329 |
Data reduction software | MOSFLM |
Data scaling software | SCALA (3.3.16) |
Refinement software | REFMAC |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 55.395 | 19.585 | 1.220 |
High resolution limit [Å] | 1.158 | 3.660 | 1.160 |
Rmerge | 0.100 | 0.138 | |
Rmeas | 0.125 | 0.169 | |
Rpim | 0.074 | 0.094 | |
Total number of observations | 407 | 11155 | |
Number of reflections | 26153 | ||
<I/σ(I)> | 8.9 | 9.4 | 6.4 |
Completeness [%] | 93.9 | 18.3 | 99.7 |
Redundancy | 2.8 | 2.2 | 2.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |