4ICB
PROLINE CIS-TRANS ISOMERS IN CALBINDIN D9K OBSERVED BY X-RAY CRYSTALLOGRAPHY
Experimental procedure
Spacegroup name | P 21 21 2 |
Unit cell lengths | 56.130, 43.000, 29.320 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 10.000 * - 1.600 |
R-factor | 0.188 |
Rwork | 0.188 |
RMSD bond length | 0.024 |
RMSD bond angle | 0.043 * |
Phasing software | X-PLOR |
Refinement software | PROFFT |
Data quality characteristics
Overall | |
High resolution limit [Å] | 1.600 * |
Rmerge | 0.067 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 8.7 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 50 (mg/ml) | |
2 | 1 | drop | Tris-HCl | 0.1 (M) | |
3 | 1 | drop | 15 (mM) | ||
4 | 1 | drop | sodium sulphate | 80 (%sat) |