4I7W
Agrobacterium tumefaciens DHDPS with lysine and pyruvate
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Wavelength(s) | 0.9536 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 89.090, 122.780, 129.640 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 40.000 - 1.300 |
R-factor | 0.17192 |
Rwork | 0.172 |
R-free | 0.18647 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.005 |
RMSD bond angle | 1.058 |
Refinement software | REFMAC (5.5.0072) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 40.000 |
High resolution limit [Å] | 1.300 |
Number of reflections | 39292 |
Completeness [%] | 97.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8.5 | 293 | 0.17 M lithium sulfate monohydrate, 0.085 M Tris pH 8.5, 25.5 % (w/v) PEG 4000, 15% (v/v) glycerol, VAPOR DIFFUSION, HANGING DROP, temperature 293K |