4I6P
Crystal structure of Par3-NTD domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-12-01 |
Detector | RAYONIX MX-225 |
Wavelength(s) | 0.979 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 108.780, 108.780, 46.730 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 39.940 - 2.900 |
R-factor | 0.23296 |
Rwork | 0.230 |
R-free | 0.29361 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2ns5 |
RMSD bond length | 0.012 |
RMSD bond angle | 1.791 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.000 |
High resolution limit [Å] | 2.900 | 2.900 |
Rmerge | 0.148 | 0.477 |
Number of reflections | 6406 | |
<I/σ(I)> | 17 | 5.3 |
Completeness [%] | 97.1 | 100 |
Redundancy | 7.6 | 7.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 289.15 | 1.6 M ammonium sulfate, 100 mM HEPES, pH 7.5, VAPOR DIFFUSION, SITTING DROP, temperature 289.15K |