4I3A
Structures of PR1 and PR2 intermediates from time-resolved laue crystallography collected at 14ID-B, APS
Experimental procedure
| Experimental method | LAUE |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 14-ID-B |
| Synchrotron site | APS |
| Beamline | 14-ID-B |
| Temperature [K] | 288 |
| Detector technology | CCD |
| Collection date | 2008-11-17 |
| Detector | MAR CCD 165 mm |
| Wavelength(s) | 0.96-1.30 |
| Spacegroup name | P 63 |
| Unit cell lengths | 66.833, 66.833, 40.947 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 10.000 - 1.600 |
| R-factor | 0.301 |
| Rwork | 0.298 |
| R-free | 0.34900 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.005 |
| RMSD bond angle | 0.013 |
| Data reduction software | LaueView |
| Data scaling software | LaueView |
| Refinement software | SHELX |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 28.900 |
| High resolution limit [Å] | 1.600 |
| Number of reflections | 14632 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7 | 298 | 2.6M AMMONIUM SULFATE, 50MM SODIUM PHOSPHATE, pH 7.0, temperature 298K, VAPOR DIFFUSION, HANGING DROP |
