4I2O
The Structure of FixK2 from Bradyrhizobium japonicum
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 90 |
Detector technology | PIXEL |
Collection date | 2011-09-13 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 0.997 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 111.330, 43.880, 70.110 |
Unit cell angles | 90.00, 90.04, 90.00 |
Refinement procedure
Resolution | 43.579 - 1.770 |
R-factor | 0.1852 |
Rwork | 0.183 |
R-free | 0.22710 |
Structure solution method | SAD |
RMSD bond length | 0.018 |
RMSD bond angle | 2.064 |
Data reduction software | XDS (package) |
Data scaling software | XDS (package) |
Phasing software | SHELXS |
Refinement software | PHENIX ((phenix.refine: 1.7.3_928)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 43.580 |
High resolution limit [Å] | 1.770 |
Number of reflections | 66510 |
Completeness [%] | 99.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6 | 277 | 0.1M BisTris, 0.1M NH4-acetate, 16-22% PEG 10000, VAPOR DIFFUSION, SITTING DROP, temperature 277K |
1 | VAPOR DIFFUSION, SITTING DROP | 6 | 277 | 0.1M BisTris, 0.1M NH4-acetate, 16-22% PEG 10000, VAPOR DIFFUSION, SITTING DROP, temperature 277K |