4I28
Binary complex of mouse TdT with ssDNA and Zn++
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-1 |
Synchrotron site | ESRF |
Beamline | ID14-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2002-11-20 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 0.9330 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 46.824, 84.799, 115.773 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 16.730 - 2.150 |
R-factor | 0.1653 |
Rwork | 0.163 |
R-free | 0.20620 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1jms |
RMSD bond length | 0.010 |
RMSD bond angle | 1.030 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | BUSTER (2.9.3) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.270 |
High resolution limit [Å] | 2.150 | 2.150 |
Rmerge | 0.080 | 0.364 |
Number of reflections | 25680 | |
<I/σ(I)> | 4.5 | |
Completeness [%] | 99.5 | 99.2 |
Redundancy | 4.5 | 4.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 20-26% PEG4000, 100 mM HEPES, 200 mM lithium chloride, pH 6.0-7.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K |