4HZI
Crystal structure of the Leptospira interrogans ATPase subunit of an orphan ABC transporter
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 110 |
Detector technology | CCD |
Collection date | 2010-02-19 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.97919 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 58.256, 92.512, 130.579 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 43.600 - 1.850 |
R-factor | 0.18464 |
Rwork | 0.184 |
R-free | 0.22232 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2ihy |
RMSD bond length | 0.013 |
RMSD bond angle | 1.559 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 43.600 | 1.950 |
High resolution limit [Å] | 1.850 | 1.850 |
Rmerge | 0.061 | 0.800 |
Number of reflections | 61082 | |
<I/σ(I)> | 18.5 | 2.3 |
Completeness [%] | 100.0 | 100 |
Redundancy | 7.5 | 6.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 291 | 1.2M ammonium sulphate, 0.1M sodium cacodylate, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 291K |