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4HXJ

Crystal structure of SH3:RGT complex

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSSRF BEAMLINE BL17U
Synchrotron siteSSRF
BeamlineBL17U
Temperature [K]100
Detector technologyCCD
Collection date2010-04-30
DetectorADSC QUANTUM 315r
Wavelength(s)0.97885
Spacegroup nameP 1 21 1
Unit cell lengths27.980, 40.830, 43.340
Unit cell angles90.00, 105.97, 90.00
Refinement procedure
Resolution29.163 - 2.000
R-factor0.1445
Rwork0.139
R-free0.19250
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1fmk
RMSD bond length0.007
RMSD bond angle1.025
Data reduction softwareMOSFLM
Data scaling softwareSCALA
Phasing softwarePHASER
Refinement softwarePHENIX ((phenix.refine))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]29.2002.080
High resolution limit [Å]2.0002.000
Rmerge0.1700.360
Number of reflections6468
<I/σ(I)>107
Completeness [%]99.0100
Redundancy88
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP8298100mM Tris, pH 8.0, 1.3M sodium citrate, VAPOR DIFFUSION, HANGING DROP, temperature 298K

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