4HX5
Crystal structure of 11 beta-HSD1 in complex with SAR184841
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9762 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 56.399, 153.491, 73.755 |
Unit cell angles | 90.00, 92.89, 90.00 |
Refinement procedure
Resolution | 73.660 - 2.190 |
Rwork | 0.163 |
R-free | 0.19940 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3qqp |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | BUSTER |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 73.660 |
High resolution limit [Å] | 2.190 |
Rmerge | 0.082 |
Number of reflections | 64258 |
<I/σ(I)> | 13.1 |
Completeness [%] | 100.0 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 277 | 40% PEG300, 0.1M MES, PH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 277K |