4HWH
Crystal structure of ATBAG4
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-05-10 |
Detector | RAYONIX MX-225 |
Wavelength(s) | 0.9795 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 63.663, 73.328, 111.634 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 24.189 - 1.895 |
R-factor | 0.2084 |
Rwork | 0.207 |
R-free | 0.23580 |
Structure solution method | SAD |
RMSD bond length | 0.005 |
RMSD bond angle | 0.609 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | SHELXS |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 24.189 | 1.940 |
High resolution limit [Å] | 1.895 | 1.895 |
Number of reflections | 40074 | |
Completeness [%] | 95.4 | 72.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5 | 293 | 10% tascimate, 20% PEG3350, pH 5.0, VAPOR DIFFUSION, HANGING DROP, temperature 293K |