4HTZ
Crystal structure of PDE2 catalytic domain in space group P1
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL17U |
| Synchrotron site | SSRF |
| Beamline | BL17U |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2012-06-27 |
| Detector | ADSC QUANTUM 315 |
| Wavelength(s) | 0.9793 |
| Spacegroup name | P 1 |
| Unit cell lengths | 56.190, 73.870, 92.610 |
| Unit cell angles | 109.68, 91.71, 90.91 |
Refinement procedure
| Resolution | 33.814 - 2.000 |
| R-factor | 0.1915 |
| Rwork | 0.188 |
| R-free | 0.24880 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.043 |
| Data reduction software | iMOSFLM |
| Phasing software | MOLREP |
| Refinement software | PHENIX ((phenix.refine: 1.7.1_743)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 33.814 |
| High resolution limit [Å] | 2.000 |
| Number of reflections | 88029 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
