4HMG

REFINEMENT OF THE INFLUENZA VIRUS HEMAGGLUTININ BY SIMULATED ANNEALING

Experimental procedure

Spacegroup name	P 41
Unit cell lengths	162.800, 162.800, 176.800
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	? - 3.000
Rwork	0.231
RMSD bond length	0.014
RMSD bond angle	2.900
Refinement software	X-PLOR

Data quality characteristics

	Overall
Low resolution limit [Å]	7.000 *
High resolution limit [Å]	3.000 *
Rmerge	0.125 *
Number of reflections	64062 *
Completeness [%]	70.8 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Microdialysis *	7.5 *		referred to 'Weis, W.', (1988) Nature, 333, 426-431 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	1	protein	35 (mg/ml)
2	1	2	Na3 citrate	1.34-1.38 (M)
3	1	2		0.1 (%)