4HKB
CH67 Fab (unbound) from the CH65-67 Lineage
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-02-17 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.97919 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 113.249, 123.269, 228.828 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 41.698 - 3.600 |
R-factor | 0.2608 |
Rwork | 0.258 |
R-free | 0.30560 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.005 |
RMSD bond angle | 1.378 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX (1.7.3_928) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 3.660 |
High resolution limit [Å] | 3.600 | 9.750 | 3.600 |
Rmerge | 0.107 | 0.039 | 0.452 |
Number of reflections | 38632 | ||
<I/σ(I)> | 6.6 | ||
Completeness [%] | 99.8 | 98.8 | 99.9 |
Redundancy | 4.8 | 4.4 | 5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 298 | 15-20% PEG4000, 10 mM Tris-HCl, pH 8, VAPOR DIFFUSION, HANGING DROP, temperature 298K |