4HHG
Crystal structure of the Pseudomonas aeruginosa azurin, RuH107NO YOH109
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL12-2 |
Synchrotron site | SSRL |
Beamline | BL12-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-02-17 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.00 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 49.762, 67.176, 81.385 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 33.590 - 1.600 |
R-factor | 0.23545 |
Rwork | 0.234 |
R-free | 0.26052 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.025 |
RMSD bond angle | 2.682 |
Data reduction software | autoXDS |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 51.810 |
High resolution limit [Å] | 1.180 |
Completeness [%] | 97.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.2 | 293.15 | 26-34% PEG 4000, 100mM Lithium Nitrate, 6.25mM Copper Sulfate and 100 mM Imidazole, pH 7.2, VAPOR DIFFUSION, SITTING DROP, temperature 293.15K |