4HGK
Shark IgNAR variable domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Temperature [K] | 298 |
Detector technology | IMAGE PLATE |
Detector | MAR scanner 300 mm plate |
Wavelength(s) | 1.0 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 127.980, 127.980, 151.760 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 52.055 - 3.040 |
R-factor | 0.2387 |
Rwork | 0.237 |
R-free | 0.26630 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ha2 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.100 |
Data reduction software | xia2 |
Data scaling software | xia2 |
Phasing software | PHASER |
Refinement software | BUSTER (2.9.3) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 52.055 |
High resolution limit [Å] | 3.040 |
Rmerge | 0.220 |
Number of reflections | 25935 |
Completeness [%] | 93.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.6 | 291 | 16% PEG 2000 MME, 100 mM sodium acetate pH 4.6, VAPOR DIFFUSION, HANGING DROP, temperature 291K |