4HCZ
PHF1 Tudor in complex with H3K36me3
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RUH3R |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2011-01-20 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.541 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 88.030, 29.670, 62.000 |
Unit cell angles | 90.00, 116.41, 90.00 |
Refinement procedure
Resolution | 23.413 - 1.850 |
R-factor | 0.2058 |
Rwork | 0.204 |
R-free | 0.24390 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2e5p |
RMSD bond length | 0.007 |
RMSD bond angle | 1.060 |
Data reduction software | d*TREK |
Data scaling software | d*TREK |
Phasing software | PHASER |
Refinement software | PHENIX (1.6.4_486) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 23.413 | 1.920 |
High resolution limit [Å] | 1.850 | 1.850 |
Number of reflections | 12091 | |
Completeness [%] | 96.4 | 81.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 277.15 | 0.1 M HEPES pH 7.5, 20% PEG 10000, VAPOR DIFFUSION, SITTING DROP, temperature 277.15K |