4HCS
Structure of Novel subfamily CX chemokine solved by sulfur SAD
Experimental procedure
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 21-ID-D |
| Synchrotron site | APS |
| Beamline | 21-ID-D |
| Wavelength(s) | 0.97924 |
| Spacegroup name | P 61 2 2 |
| Unit cell lengths | 44.640, 44.640, 142.190 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 22.908 - 1.280 |
| R-factor | 0.1843 |
| Rwork | 0.183 |
| R-free | 0.20610 |
| Structure solution method | SAD |
| RMSD bond length | 0.005 |
| RMSD bond angle | 1.013 |
| Refinement software | PHENIX ((phenix.refine: 1.8_1069)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 23.000 |
| High resolution limit [Å] | 1.280 |
| Number of reflections | 21906 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7 | 298 | 2.4 M Sodium Malonate, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 298K |
