4H9S

Complex structure 6 of DAXX/H3.3(sub7)/H4

Experimental procedure

Source type	SYNCHROTRON
Source details	NSLS BEAMLINE X29A
Synchrotron site	NSLS
Beamline	X29A
Wavelength(s)	1.075
Spacegroup name	P 21 21 21
Unit cell lengths	96.397, 99.165, 100.611
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	44.092 - 2.600
R-factor	0.198
Rwork	0.195
R-free	0.25030
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.005
RMSD bond angle	0.939
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHASER
Refinement software	PHENIX ((phenix.refine: 1.7.2_869))

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	2.600
Rmerge	0.075
Number of reflections	30321
<I/σ(I)>	36.7
Completeness [%]	99.9
Redundancy	7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	6.2	293	0.1 M Na/K-phosphate, 2.5M NaCl, pH 6.2, VAPOR DIFFUSION, HANGING DROP, temperature 293K