4H9O

Complex structure 2 of DAXX/H3.3(sub5,G90M)/H4

Experimental procedure

Source type	SYNCHROTRON
Source details	APS BEAMLINE 24-ID-E
Synchrotron site	APS
Beamline	24-ID-E
Wavelength(s)	0.979
Spacegroup name	P 43 21 2
Unit cell lengths	107.691, 107.691, 90.766
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	38.075 - 2.053
R-factor	0.1843
Rwork	0.182
R-free	0.22450
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.008
RMSD bond angle	1.005
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHASER
Refinement software	PHENIX ((phenix.refine: 1.7.2_869))

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	2.050
Number of reflections	33889
Completeness [%]	99.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	7	277	1.8 M Na/K-phosphate, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 277K