4GTM
FTase in complex with BMS analogue 11
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-12-12 |
Detector | MARMOSAIC 225 mm CCD |
Wavelength(s) | 0.9789 |
Spacegroup name | P 61 |
Unit cell lengths | 173.171, 173.171, 70.289 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 19.940 - 2.200 |
R-factor | 0.17552 |
Rwork | 0.173 |
R-free | 0.21782 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3eu5 |
RMSD bond length | 0.014 |
RMSD bond angle | 1.410 |
Data reduction software | MOSFLM |
Data scaling software | XSCALE |
Phasing software | PHASES |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.940 | 2.260 |
High resolution limit [Å] | 2.200 | 2.200 |
Number of reflections | 61202 | |
<I/σ(I)> | 20.9 | 4.6 |
Completeness [%] | 99.9 | 100 |
Redundancy | 6.2 | 6.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 292 | 20% (w/v) PEG 4000, 0.2M MgCl2, 0.1M Tris , pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 292K |