4GR1

THE BINDING OF THE RETRO-ANALOGUE OF GLUTATHIONE DISULFIDE TO GLUTATHIONE REDUCTASE

Experimental procedure

Spacegroup name	B 1 1 2
Unit cell lengths	119.800, 84.500, 63.200
Unit cell angles	90.00, 90.00, 58.70

Refinement procedure

Resolution	? - 2.400
R-factor	0.151
Refinement software	TNT

Data quality characteristics

	Overall
High resolution limit [Å]	2.400 *
Number of reflections	21690 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *			referred to J.Mol.Biol.152.763-782 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	enzyme	0.15 (mM)
2	1	reservoir	ammonium sulfate	0.8 (M)
3	1	drop	ammonium sulfate	1.2 (M)