4GPD

THE STRUCTURE OF LOBSTER APO-D-GLYCERALDEHYDE-3-PHOSPHATE DEHYDROGENASE AT 3.0 ANGSTROMS RESOLUTION

Replaces:  2GPD

Experimental procedure

Spacegroup name	P 1
Unit cell lengths	83.019, 80.956, 82.545
Unit cell angles	110.85, 71.47, 116.86

Refinement procedure

Resolution	6.000 - 3.000 *
R-factor	0.218
Refinement software	PROLSQ

Data quality characteristics

	Overall
High resolution limit [Å]	3.000 *
Total number of observations	56899 *
Number of reflections	30128 *
Completeness [%]	86.0 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	1	protein	18 (mg/ml)
2	1	2	ammonium sulfate	3.08 (M)
3	1	2	EDTA	1 (mM)
4	1	2	dithiothreitol	1 (mM)
5	1	2	chloroform		dialyzing medium