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4GOX

Sulfotransferase Domain from the Synechococcus PCC 7002 Olefin Synthase

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 23-ID-D
Synchrotron siteAPS
Beamline23-ID-D
Temperature [K]100
Detector technologyCCD
Collection date2010-07-15
DetectorMARMOSAIC 300 mm CCD
Wavelength(s)0.97934
Spacegroup nameP 42 21 2
Unit cell lengths131.440, 131.440, 47.080
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution33.070 - 2.150
R-factor0.1898
Rwork0.188
R-free0.21970
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.010
RMSD bond angle1.060
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwarePHASER
Refinement softwareBUSTER (2.10.0)
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]50.00050.0002.230
High resolution limit [Å]2.1504.6302.150
Rmerge0.0350.633
Number of reflections23099
Completeness [%]99.898.4100
Redundancy87.5
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP629327-30% PEG1500, 100 mM MMT buffer (DL-malic acid, MES, Tris), pH 6.0, VAPOR DIFFUSION, HANGING DROP, temperature 293K

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