4GOQ
Crystal structure of a DUF1491 family protein (CC_1065) from Caulobacter crescentus CB15 at 1.87 A resolution
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL11-1 |
Synchrotron site | SSRL |
Beamline | BL11-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-06-28 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97849,0.91837,0.97898 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 59.730, 59.730, 323.010 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 49.262 - 1.870 |
R-factor | 0.1818 |
Rwork | 0.180 |
R-free | 0.21060 |
Structure solution method | MAD |
RMSD bond length | 0.010 |
RMSD bond angle | 0.890 |
Data reduction software | XDS |
Data scaling software | XSCALE (March 15, 2012) |
Phasing software | SHELX |
Refinement software | BUSTER-TNT (2.10.0) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 49.262 | 49.260 | 1.940 |
High resolution limit [Å] | 1.870 | 4.020 | 1.870 |
Rmerge | 0.075 | 0.032 | 0.902 |
Number of reflections | 56900 | 6150 | 5785 |
<I/σ(I)> | 16.3 | 45.8 | 2.27 |
Completeness [%] | 99.7 | 99.2 | 99.5 |
Redundancy | 6.45 | 6.52 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 293 | 0.2M magnesium chloride, 2.5M sodium chloride, 0.1M TRIS pH 7.0, NANODROP, VAPOR DIFFUSION, SITTING DROP, temperature 293K |