4GN4
OBody AM2EP06 bound to hen egg-white lysozyme
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2010-09-02 |
Detector | MAR 2300 |
Wavelength(s) | 1.54179 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 50.430, 58.330, 81.820 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 81.820 - 1.861 |
R-factor | 0.1541 |
Rwork | 0.152 |
R-free | 0.19440 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.026 |
RMSD bond angle | 1.948 |
Data reduction software | MOSFLM |
Data scaling software | SCALA (3.3.16) |
Phasing software | PHASER (2.1.4) |
Refinement software | REFMAC |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 81.820 | 34.575 | 1.960 |
High resolution limit [Å] | 1.861 | 5.880 | 1.861 |
Rmerge | 0.027 | 0.226 | |
Total number of observations | 4073 | 18275 | |
Number of reflections | 20797 | ||
<I/σ(I)> | 29.2 | 15.7 | 3.4 |
Completeness [%] | 99.1 | 99.4 | 94.1 |
Redundancy | 6.9 | 5.4 | 6.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 291 | 0.2 M HEPES, 13% MPEG5000, pH 7.0, VAPOR DIFFUSION, SITTING DROP, temperature 291K |