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4GJH

Crystal Structure of the TRAF domain of TRAF5

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsPHOTON FACTORY BEAMLINE BL-5A
Synchrotron sitePhoton Factory
BeamlineBL-5A
Temperature [K]77
Detector technologyCCD
Collection date2010-06-06
DetectorADSC QUANTUM 210r
Wavelength(s)1.000
Spacegroup nameP 21 21 21
Unit cell lengths71.052, 90.579, 117.216
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution33.073 - 2.805
R-factor0.227
Rwork0.224
R-free0.27310
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.011
RMSD bond angle1.156
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwareMLPHARE
Refinement softwarePHENIX ((phenix.refine: 1.6.4_486))
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]50.00050.0002.850
High resolution limit [Å]2.8007.5902.800
Number of reflections17854
Completeness [%]93.898100
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP6.52890.1M Bis-Tris, 15%(w/v) PEG10000, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 289K

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