4GGG
Crystal structure of V66A/L68V CzrA in the Zn(II)bound state.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RUH3R |
Temperature [K] | 113 |
Detector technology | IMAGE PLATE |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.5418 |
Spacegroup name | P 21 2 21 |
Unit cell lengths | 46.286, 50.198, 85.877 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 26.669 - 1.998 |
R-factor | 0.1778 |
Rwork | 0.173 |
R-free | 0.22430 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1r1v |
RMSD bond length | 0.005 |
RMSD bond angle | 0.803 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX ((phenix.refine: 1.7.1_743)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 26.669 | 2.030 |
High resolution limit [Å] | 1.998 | 2.000 |
Number of reflections | 13543 | |
Completeness [%] | 91.5 | 94.2 |
Redundancy | 5.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 9.5 | 293 | PEG 8000, NaCl, Ches, pH 9.5, VAPOR DIFFUSION, HANGING DROP, temperature 293 K, temperature 293.K |