4GF3
Structure of a SycH-YopH Chaperone-Effector Complex
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | NSLS BEAMLINE X29A |
| Synchrotron site | NSLS |
| Beamline | X29A |
| Temperature [K] | 93.15 |
| Wavelength(s) | 1.0084 |
| Spacegroup name | P 41 21 2 |
| Unit cell lengths | 70.525, 70.525, 71.517 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 31.540 - 1.900 |
| R-factor | 0.18266 |
| Rwork | 0.180 |
| R-free | 0.24481 |
| Structure solution method | SAD |
| RMSD bond length | 0.018 |
| RMSD bond angle | 1.890 |
| Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 31.540 |
| High resolution limit [Å] | 1.900 |
| Number of reflections | 13866 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
