4GC5

Crystal structure of murine TFB1M

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	NSLS BEAMLINE X29A
Synchrotron site	NSLS
Beamline	X29A
Temperature [K]	100
Detector technology	CCD
Collection date	2011-02-01
Detector	ADSC QUANTUM 315r
Wavelength(s)	0.9790
Spacegroup name	I 2 2 2
Unit cell lengths	47.630, 101.270, 211.660
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	33.418 - 1.801
R-factor	0.1863
Rwork	0.184
R-free	0.22360
RMSD bond length	0.013
RMSD bond angle	1.515
Data reduction software	XDS
Data scaling software	SCALA
Phasing software	SHARP
Refinement software	PHENIX ((phenix.refine: 1.8_1069))

Data quality characteristics

	Overall
Low resolution limit [Å]	40.000
High resolution limit [Å]	1.801
Number of reflections	33212

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	7	277	2.9 M Sodium Acetate, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 277K