4G8W
Rat Heme Oxygenase-1 in complex with Heme and O2 with 13 hr illumination: Laser on
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 14-BM-C |
Synchrotron site | APS |
Beamline | 14-BM-C |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-04-25 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.979 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 65.300, 65.300, 121.465 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 28.760 - 2.400 |
R-factor | 0.16868 |
Rwork | 0.166 |
R-free | 0.22833 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 4g8u |
RMSD bond length | 0.016 |
RMSD bond angle | 2.223 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | REFMAC (5.6.0117) |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.440 |
High resolution limit [Å] | 2.400 | 2.400 |
Number of reflections | 12112 | |
<I/σ(I)> | 9.4 | |
Completeness [%] | 98.7 | 99.2 |
Redundancy | 3.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 293 | 4M sodium formate, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 293K |