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4G6V

CdiA-CT/CdiI toxin and immunity complex from Burkholderia pseudomallei

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsALS BEAMLINE 8.2.1
Synchrotron siteALS
Beamline8.2.1
Temperature [K]100
Detector technologyCCD
Collection date2011-06-11
DetectorADSC QUANTUM 315r
Wavelength(s)0.92
Spacegroup nameF 2 2 2
Unit cell lengths151.963, 173.654, 174.822
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution43.400 - 2.640
R-factor0.2065
Rwork0.204
R-free0.24520
Structure solution methodSAD
RMSD bond length0.010
RMSD bond angle1.186
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwarePHENIX
Refinement softwarePHENIX ((phenix.refine: 1.7.1_743))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]43.4002.740
High resolution limit [Å]2.6402.640
Number of reflections34071
Completeness [%]99.5100
Redundancy29.630.1
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP7.22980.49 M sodium phosphate monobasic, 0.96 M potassium phosphate dibasic, 10 mM triethylene glycol, 504 nM chymotrypsin, pH 7.2, VAPOR DIFFUSION, HANGING DROP, temperature 298K

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