4G65
Potassium transporter peripheral membrane component (trkA) from Vibrio vulnificus
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 21-ID-G |
Synchrotron site | APS |
Beamline | 21-ID-G |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-06-30 |
Detector | MARMOSAIC 300 mm CCD |
Wavelength(s) | 0.97856 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 68.112, 225.256, 139.516 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.670 - 2.090 |
R-factor | 0.18108 |
Rwork | 0.179 |
R-free | 0.22781 |
Structure solution method | SAD |
RMSD bond length | 0.013 |
RMSD bond angle | 1.613 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.140 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.087 | 0.610 |
Number of reflections | 63411 | |
<I/σ(I)> | 20.9 | 3.3 |
Completeness [%] | 99.9 | 100 |
Redundancy | 6.7 | 6.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | 1.3M NH4Tartr 0.1M Hepes, 0.3M NDSB211, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 293K |