4FX2

COMPARISON OF THE CRYSTAL STRUCTURES OF A FLAVODOXIN IN ITS THREE OXIDATION STATES AT CRYOGENIC TEMPERATURES

Experimental procedure

Spacegroup name	P 43 21 2
Unit cell lengths	51.440, 51.440, 139.620
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	? - 1.900
R-factor	0.203
RMSD bond length	0.034
RMSD bond angle	0.060 *
Refinement software	PROLSQ

Data quality characteristics

	Overall
Low resolution limit [Å]	9999.000 *
High resolution limit [Å]	1.900 *
Rmerge	0.100 *
Total number of observations	60332 *
Number of reflections	13507 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	reservoir	ammonium sulfate	3.2 (M)
2	1	reservoir	Tris-HCl	0.1 (M)
3	1	drop	protein	0.7-0.9 (%)