4FUQ
Crystal structure of apo MatB from Rhodopseudomonas palustris
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 19-ID |
Synchrotron site | APS |
Beamline | 19-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-12-02 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.979206 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 133.872, 58.813, 138.957 |
Unit cell angles | 90.00, 91.66, 90.00 |
Refinement procedure
Resolution | 24.909 - 1.702 |
R-factor | 0.16 |
Rwork | 0.158 |
R-free | 0.19670 |
Structure solution method | SAD |
RMSD bond length | 0.006 |
RMSD bond angle | 1.008 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHENIX |
Refinement software | PHENIX (1.6_289) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 30.000 | 30.000 | 1.730 |
High resolution limit [Å] | 1.700 | 4.610 | 1.700 |
Rmerge | 0.089 | 0.080 | 0.483 |
<I/σ(I)> | 33.96 | 3.5 | |
Completeness [%] | 97.1 | 97.8 | 95.5 |
Redundancy | 4.2 | 4 | 3.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 298 | 100 mM Bis-Tris pH 6.5, 84 mM MgSO4, 19.5 % (w/v) monomethyl polyethylene glycol 2000, VAPOR DIFFUSION, HANGING DROP, temperature 298K |