4FU9
Crystal Structure of the Urokinase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 160 |
Detector technology | IMAGE PLATE |
Detector | RIGAKU RAXIS II |
Wavelength(s) | 1.5418 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 55.100, 52.400, 80.250 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 18.990 - 1.600 |
R-factor | 0.152 |
Rwork | 0.150 |
R-free | 0.18200 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.130 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | BUSTER-TNT (BUSTER 2.11.1) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 40.000 | 40.000 | 1.640 |
High resolution limit [Å] | 1.600 | 3.940 | 1.600 |
Rmerge | 0.080 | 0.050 | 0.340 |
Number of reflections | 30737 | ||
<I/σ(I)> | 6.2 | ||
Completeness [%] | 97.9 | 94.8 | 86.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | 0.15 M Li2SO4, 20% polyethylene glycol MW 4000 in succinate buffer, pH 4.8-6.0, VAPOR DIFFUSION, HANGING DROP, temperature 291 - 298.0K |