Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CHESS BEAMLINE A1 |
Synchrotron site | CHESS |
Beamline | A1 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC QUANTUM 315 |
Spacegroup name | H 3 |
Unit cell lengths | 327.660, 327.660, 774.490 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 40.000 - 2.700 |
Rwork | 0.240 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | Wild-type FHV coordinates (from 1992) |
RMSD bond length | 0.007 |
RMSD bond angle | 1.466 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | GLRF |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 2.800 |
High resolution limit [Å] | 2.700 | 2.700 |
Rmerge | 0.105 | 0.824 |
Number of reflections | 709014 | |
<I/σ(I)> | 9 | 1 |
Completeness [%] | 83.5 | 53.9 |
Redundancy | 2.3 | 1.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7.5 | 295 | 5-6% PEG 8K, 0.15M LITHIUM SULFATE, 0.1M HEPES AND 0.01M CALCIUM CHLORIDE, pH 7.5, VAPOR DIFFUSION, temperature 295K |